RT Book, Section T1 Thermal decomposition of single hydroxychlorides of nickel, copper and cobalto A1 García Martínez, O. A1 López Delgado, Aurora A1 Millán, P. A1 López De Andrés, María Sol A1 Rojas López, Rosa María A1 Tigeras, P. AB The thermal decomposition reactions of Ni(OH)Cl.l½H20 in still air and in nitrogen and β-CO2(OH)3Cl and γ-Cu2(OH)3Cl in nitrogen atmosphere, have been studied by DTA and TG analysis, and the intermediates and final products have been characterized by x-ray diffraction and infrared spectroscop. The thermal evolution ot the above indicated compounds under dynamic vacuum conditions has be en studied with the aid of an x-ray high teaperature diffraction chamber. They reveals that in these conditions, the pure metallic nickel, copper and cobalt can be obtained at comparative low temperature. The infrared spectra of thése hydroxychlorides have been tentatively assigned. PB (s.n) YR 1985 FD 1985 LK https://hdl.handle.net/20.500.14352/65386 UL https://hdl.handle.net/20.500.14352/65386 LA eng DS Docta Complutense RD 10 abr 2025