RT Journal Article
T1 Bone mineral change during experimental calcination: an X-ray diffraction study
A1 Galeano, Sergio
A1 García Lorenzo, Mari Luz
AB The effects of calcination (400-1200°C) on pig bones have been studied using powder X-ray diffraction (XRD) and secondary modifications, such as color change and weight loss. The characterisation by powder XRD confirmed the presence of the crystalline phase of hydroxyapatite, and comparison of the results obtained at different temperatures suggested that at 650°C, all the organic components and carbonate substitutions were completely removed. Accordingly, these samples were white. In addition, the crystallinity degree and the crystallite size progressively increased with the calcination temperature until 650°C, remaining stable until 1200°C. Below 650°C, bone samples presented organic compounds, resulting in background noise in the diffractogram and gray or black color. In addition, impurities in the lattice correspond to low crystallite sizes.
PB Wiley
SN 1556-4029
YR 2014
FD 2014
LK https://hdl.handle.net/20.500.14352/34269
UL https://hdl.handle.net/20.500.14352/34269
LA eng
DS Docta Complutense
RD 8 may 2024