RT Journal Article T1 Assessment of ph value and release of calcium ions in calcium silicate cements: an in vitro comparative study A1 Herrera Trinidad, Rubén A1 Molinero Mourelle, Pedro A1 Fonseca, Manrique A1 Weber, Adrian Roman A1 Vera González, Vicente A1 Mena Fernández, María Luz AB AbstractThe goal of this study was to evaluate the pH and the release of calcium from four calcium-silicate-based cements.Methods: Four materials were tested (ProClinic MTA; Angelus MTA; ProRoot MTA; Biodentine). The palatal canal root of acrylic upper molars was filled with each cement. Afterwards, they were set in phosphate-buffered saline. Measurements were taken by atomic adsorption spectroscopy (AAS) at 3, 24, 72, 168, 336, 672, and 1008 h. The pH was measured at the same timepoints. Kruskal-Wallis tests were carried out in each period, as the Kolmogorov-Smirnov and Shapiro-Wilk tests showed no parametric results.Results: Significant differences (p < 0.05) in calcium release were found at the 3-, 24-, and 72-hour evaluations. All of the analyzed groups presented a release of calcium ions up to 168 h, and the general tendency was to increase up to 672 h, with a maximum release of 25.45 mg/g in the ProRoot group. We could only observe significant differences (p < 0.05) in pH value over 168 h between the Biodentine (7.93) and Angelus MTA (7.31) groups.Conclusions: There were significant differences (p < 0.05) in calcium release. Nevertheless, no significant differences (p > 0.05) in the pH values were found at the studied timepoints, except for the values at 168 h. PB MDPI YR 2023 FD 2023-09-14 LK https://hdl.handle.net/20.500.14352/103734 UL https://hdl.handle.net/20.500.14352/103734 LA eng NO Herrera-Trinidad R, Molinero-Mourelle P, Fonseca M, Weber AR, Vera V, Mena ML, Vera-González V. Assessment of pH Value and Release of Calcium Ions in Calcium Silicate Cements: An In Vitro Comparative Study. Materials (Basel). 2023 Sep 14;16(18):6213 NO 2023 Descuentos MDPI DS Docta Complutense RD 8 abr 2025