RT Journal Article T1 Ultrasensitive NO_(2 )gas sensor with insignificant NH3-interference based on a few-layered mesoporous graphene A1 Matatagui Cruz, Daniel A1 López Sánchez, Jesús A1 Peña Moreno, Álvaro A1 Serrano, Aída A1 Del Campo, Adolfo A1 Rodríguez De La Fuente, Óscar A1 Carmona Tejero, Noemí A1 Navarro Palma, Elena A1 Marín Palacios, María Pilar A1 Horrillo, María del Carmen AB Few-layered mesoporous graphene (FLMG) is employed as a sensing material to develop an innovative and high-sensitivity room temperature NO_(2) sensor through a simple manufacturing process. For this purpose, sensing material is optimized at 100 min by a high-energy milling process where natural graphite is used as a precursor: it is an inexpensive, sustainable and suitable active material. The large number of defects created and the enhanced degree of mesoporosity produced during the milling process determine the physical principles of operation of the designed device. NO_(2) gas sensing tests reveal an improved and selective performance with a change in resistance of ∼16 % at 0.5 ppm under ultraviolet photo-activation, establishing a detection limit around ∼25 ppb. Interestingly, the response of the developed sensor to humidity is independent in the measured range (0–33 % relative humidity at 25 °C) and the dependency to the presence of NH3 is rather poor as well (∼1.5 % at 50 ppm). PB Elsevier YR 2021 FD 2021 LK https://hdl.handle.net/20.500.14352/91643 UL https://hdl.handle.net/20.500.14352/91643 LA eng NO Matatagui, D., López-Sánchez, J., Peña, A., Serrano, A., Del Campo, A., De La Fuente, O.R., Carmona, N., Navarro, E., Marín, P., Del Carmen Horrillo, M.: Ultrasensitive NO2 gas sensor with insignificant NH3-interference based on a few-layered mesoporous graphene. Sensors and Actuators B: Chemical. 335, 129657 (2021). https://doi.org/10.1016/j.snb.2021.129657 NO Ministerio de Ciencia, Innovación y Universidades (España) NO Agencia Estatal de Investigación (España) NO European Commission NO Comunidad de Madrid DS Docta Complutense RD 26 abr 2025