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Negishi reaction in BODIPY dyes. Unprecedented alkylation by palladium-catalyzed C–C coupling in boron dipyrromethene derivatives

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https://doi.org/10.1039/c4ra00651h

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2014

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Royal Society of Chemistry
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https://hdl.handle.net/20.500.14352/98895

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Durán Sampedro, G., Palao, E., Rodríguez Agarrabeitia, A. et al. «Negishi Reaction in BODIPY Dyes. Unprecedented Alkylation by Palladium-Catalyzed C–C Coupling in Boron Dipyrromethene Derivatives». RSC Adv., vol. 4, n.o 37, 2014, pp. 19210-13. https://doi.org/10.1039/C4RA00651H.

Abstract

Negishi reactions of 3-halogen and 3,5-dihalogen substituted BODIPYs with different organozinc reagents are reported as the first examples of this valuable palladium-catalyzed C–C coupling reaction into the family of the BODIPY dyes. It is demonstrated that the Negishi coupling is especially useful for obtaining interesting alkylated BODIPYs, including synthetically-valuable asymmetrically-3,5-disubstituted BODIPYs.

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Química orgánica (Química)

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22 Física, 23 Química, 33 Ciencias Tecnológicas

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